Xylem ProLab 1000 User Manual

OPERATING MANUALba75576e05 11/2013ProLab 1000 pH/ISEMEASURING INSTRUMENT WITH AUTOMATIC SENSOR RECOGNITION AND ELECTRONIC ACCESS CONTROLMENUOK

Overview ProLab 100010ba75576e05 11/20131.4 Socket fieldCAUTIONOnly connect sensors to the meter that cannot return any voltages or currents that are

ProLab 1000100ba75576e05 11/2013A.2.6 pH/UpH/U (<MENU/OK>)– Calibration– Calibration record– Calibration history– Buffer– NIST/DIN– TEC–Merck 1–

ProLab 1000101ba75576e05 11/2013A.2.7 ISEISE (<MENU/OK>)– Calibration record– Calibration history– Man. temperature : -20 ... +130 °C– Ion type–

ProLab 1000102ba75576e05 11/2013

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ProLab 1000 Overview11ba75576e05 11/20131.5 Automatic sensor recognitionThe automatic sensor recognition function enables  to operate a sensor with d

Overview ProLab 100012ba75576e05 11/2013ID sensors SI Analytics ID sensors support the automatic sensor recognition function. Their sensor designation

ProLab 1000 Overview13ba75576e05 11/20131.6 Electronic access controlThe ProLab 1000 always documents measurement data and calibration data with an ID

Overview ProLab 100014ba75576e05 11/2013

ProLab 1000 Safety15ba75576e05 11/20132 SafetyThis operating manual contains basic instructions that you must follow during the commissioning, operati

Safety ProLab 100016ba75576e05 11/20132.2 General safety instructionsThis instrument is built and inspected according to the relevant guidelines and n

ProLab 1000 Commissioning17ba75576e05 11/20133 Commissioning3.1 Scope of delivery ProLab 1000 laboratory meter Power pack 4 batteries 1.5 V Micro t

Commissioning ProLab 100018ba75576e05 11/20133.3 Initial commissioningPerform the following activities: Insert the batteries (see page 77) Connect t

ProLab 1000 Operation19ba75576e05 11/20134 Operation4.1 Switch the meter on and offSwitching onSwitching off1 Press the <On/Off> key.The display

2 ba75576e05 11/2013ProLab 1000CE conformityRadio data transmissionSI Analytics GmbH hereby declares that the ProLab 1000 meter is in compliance with

Operation ProLab 100020ba75576e05 11/20134.2 General operating principlesThis section contains basic information on the operation of the ProLab 1000.

ProLab 1000 Operation21ba75576e05 11/20134.2.2 NavigationMeasured value display In the measured value display, you can  open the relevant measuring m

Operation ProLab 100022ba75576e05 11/2013 FunctionsFunctions are indicated by the name of the function. They are immediately carried out by confirmin

ProLab 1000 Operation23ba75576e05 11/20134.2.3 Navigation example 1: Setting the language1 Switch on the meter (see page 19)2 In the measured value di

Operation ProLab 100024ba75576e05 11/20135 Select the General submenu with <▲><▼>.The current selection is displayed in a frame.6 Open the

ProLab 1000 Operation25ba75576e05 11/20134.2.4 Navigation example 2: Setting the date and timeThe meter has a clock with a date function. The date and

Operation ProLab 100026ba75576e05 11/20135 Change and confirm the setting with <▲><▼> and <MENU/OK>.The hours are highlighted.6 Chan

ProLab 1000 Operation27ba75576e05 11/20134.3 Access controlWhen the meter is delivered, only the enclosed electronic administrator key has an access a

Operation ProLab 100028ba75576e05 11/2013Adding new USER IDsDisplaying registeredUSER IDsErasing a registeredUSER IDOutputting a list of theregistered

ProLab 1000 Operation29ba75576e05 11/20134.3.2 Lost your electronic key?Without an electronic key with access authorization, anonymous access is possi

ba75576e05 11/2013 3ProLab 1000KONFORMITÄTSERKLÄRUNGDECLARATION OF CONFORMITYDÉCLARATION DE CONFORMITÉWir erklären in alleiniger Verantwortung, dass d

Operation ProLab 100030ba75576e05 11/20134.4 System settings (system menu)The system menu comprises the following settings: Data storage (see page 30

ProLab 1000 Operation31ba75576e05 11/20134.4.3 SystemOverview The following sensor-independent meter features can be adjusted in the system menu/Syste

Operation ProLab 100032ba75576e05 11/20134.4.4 Automatic Stability controlThe automatic Stability control function continuously checks the stability o

ProLab 1000 Operation33ba75576e05 11/20134.5 pH value / ORP voltage4.5.1 General informationYou can measure the following variables: pH value [ ] OR

Operation ProLab 100034ba75576e05 11/20134.5.2 Measuring the pH valueStability control The Stability control function checks the stability of the meas

ProLab 1000 Operation35ba75576e05 11/2013Criteria With identical measurement conditions, the following applies:4 Using <SC> or <MODE>, rel

Operation ProLab 100036ba75576e05 11/20134.5.3 Measuring the ORPNoteORP electrodes are not calibrated. However, you can check ORP electrodes using a t

ProLab 1000 Operation37ba75576e05 11/2013Criteria With identical measurement conditions, the following applies:4 Using <SC> or <MODE>, rel

Operation ProLab 100038ba75576e05 11/20134.5.4 Settings for pH and ORP measurementsOverview The following settings are possible for pH and ORP measure

ProLab 1000 Operation39ba75576e05 11/2013Man. temperature -20 ... +130 °C Entry of the manually determined temperature. For measurements without tempe

4 ba75576e05 11/2013ProLab 1000

Operation ProLab 100040ba75576e05 11/20134.5.5 pH calibrationWhy calibrate? pH electrodes age. This changes the zero point (asymmetry) and slope of th

ProLab 1000 Operation41ba75576e05 11/20138 DIN 19267 1.0904.6506.7909.23025 °C9 Mettler US * 1.6794.0037.00210.01325 °C10 Mettler EU * 1.9954.0057.002

Operation ProLab 100042ba75576e05 11/20138 DIN 19267 1.0904.6506.7909.23025 °C9 Mettler US * 1.6794.0037.00210.01325 °C10 Mettler EU * 1.9954.0057.002

ProLab 1000 Operation43ba75576e05 11/2013 * Brand names or trade names are trademarks of their respective owners protected by law (see page 91).NoteT

Operation ProLab 100044ba75576e05 11/2013Calibration points Calibration can be performed using one to five buffer solutions in any order (single-point

ProLab 1000 Operation45ba75576e05 11/2013Sample record:Calibration evaluation After calibrating, the meter automatically evaluates the calibration. Th

Operation ProLab 100046ba75576e05 11/20134.5.6 Calibration intervalThe calibration interval and calibration evaluation are indicated on the display as

ProLab 1000 Operation47ba75576e05 11/20134.5.7 CalibratingMake sure the Buffer setting is correctly set in the sensor menu (see page 38).Use any one t

Operation ProLab 100048ba75576e05 11/2013NoteFor single-point calibration, the meter uses the Nernst slope (-59.16 mV/pH at 25 °C) and determines the

ProLab 1000 Operation49ba75576e05 11/2013Continuing with three-point to five-pointcalibration(Buffer NIST/DIN)12 Wait for the measurement with stabili

ProLab 1000 Contents5ba75576d05 11/20131 Overview . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 71.1 General features

Operation ProLab 100050ba75576e05 11/2013NoteAfter a five-point calibration the calibration procedure is automatically terminated. The menu item Termi

ProLab 1000 Operation51ba75576e05 11/20134.5.8 Measurements with dead stop functionMeasurements with dead stop function are normally used for measured

Operation ProLab 100052ba75576e05 11/20134.6 Ion concentration4.6.1 General informationNoteIncorrect calibration of ion sensitive electrodes will resu

ProLab 1000 Operation53ba75576e05 11/2013Preparatory activities Perform the following preparatory activities when you want to measure:NoteWhile no val

Operation ProLab 100054ba75576e05 11/2013NoteYou can terminate prematurely the manual Stability control function with <MENU/OK> manually at any

ProLab 1000 Operation55ba75576e05 11/20134.6.4 Calibrating for ISE measurementsWhy calibrate? Ion-selective electrodes age and are temperature-depende

Operation ProLab 100056ba75576e05 11/2013NoteThe measurement precision is also dependent on the selected standard solutions. Therefore, the selected s

ProLab 1000 Operation57ba75576e05 11/2013NoteThe calibration record is automatically transmitted to the interface after calibrating.Sample record:Cali

Operation ProLab 100058ba75576e05 11/20132 Start the calibration with <CAL>.The calibration display appears.3 Thoroughly rinse the electrode wit

ProLab 1000 Operation59ba75576e05 11/2013Continuing with two-point calibration[i] #1 0.010 mg/l 24 °C[i] Immerse sensor in std. 2Set temperature:24 °C

Contents ProLab 10006ba75576d05 11/20134.7 Storage . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 614.7.1 Manual storage

Operation ProLab 100060ba75576e05 11/2013Continuing with three-point to seven-pointcalibrationRepeat the steps 12 to 20 in the same way with the third

ProLab 1000 Operation61ba75576e05 11/20134.7 StorageYou can transmit measured values (datasets) to the data storage in two ways: Manual storage (see

Operation ProLab 100062ba75576e05 11/20134.7.1 Manual storageProceed as follows to transmit to the data storage and simultaneously download to the int

ProLab 1000 Operation63ba75576e05 11/20134.7.2 Automatic storage at intervalsThe storage interval (Interval) determines the chronological interval bet

Operation ProLab 100064ba75576e05 11/2013Data storageadministrationThe two lower display lines indicate the use of the data storage calculated in adva

ProLab 1000 Operation65ba75576e05 11/2013Terminating theautomatic storagefunction prematurelyProceed as follows to switch off the automatic storage fu

Operation ProLab 100066ba75576e05 11/2013SettingsMenu item Setting/functionDescriptionData storage / Manual data storage / Display- Displays in pages

ProLab 1000 Operation67ba75576e05 11/2013Data filterDisplay presentationof a datasetSample printoutMenu item Setting/functionDescriptionFilter Filter

Operation ProLab 100068ba75576e05 11/2013Quitting the display To quit the display of stored measuring datasets, you have the following options: Switc

ProLab 1000 Operation69ba75576e05 11/2013Sample printoutMenu item Setting/functionDescriptionData storage / Calibration data storage /Display- Display

ProLab 1000 Overview7ba75576e05 11/20131Overview1.1 General featuresThe ProLab 1000 precision pH meter enables you to perform pH, ORP and ion-selecti

Operation ProLab 100070ba75576e05 11/20134.7.6 Displaying and downloading calibration historyYou can display and then output to the interface the cali

ProLab 1000 Operation71ba75576e05 11/20134.8 Transmitting data (to a PC or printer)The meter has two interfaces:  RS232 interface (serial port) USB

Operation ProLab 100072ba75576e05 11/2013Socket assignment(RS232)4.8.2 USB interface (device)Connect the interface to the PC via the supplied Z875 USB

ProLab 1000 Operation73ba75576e05 11/20134.8.3 Options for data transmissionVia the RS232 interface, you can transmit data to a PC or external printer

Operation ProLab 100074ba75576e05 11/20134.8.4 Operation with MultiLab pilotWith the aid of the MultiLab pilot software, you can record and evaluate m

ProLab 1000 Operation75ba75576e05 11/20134.9.2 Resetting the system settingsThe following system settings can be reset to the delivery status:The syst

Operation ProLab 100076ba75576e05 11/2013

ProLab 1000 Maintenance, cleaning, disposal77ba75576e05 11/20135 Maintenance, cleaning, disposal5.1 MaintenanceThe only maintenance activity required

Maintenance, cleaning, disposal ProLab 100078ba75576e05 11/2013CAUTIONMake sure that the poles of the batteries are the right way round.The ± signs on

ProLab 1000 What to do if...79ba75576e05 11/20136 What to do if...6.1 pH and ORP measurementError messageErr1Error messageErr2Error messageErr4Error m

Overview ProLab 10008ba75576e05 11/20131.2 KeypadIn this operating manual, keys are indicated by brackets <..> . The key symbol (e.g. <MENU/O

What to do if... ProLab 100080ba75576e05 11/2013No stable measuredvalue Obviously incorrectmeasured valuesBuffer solutions:– Incorrect buffer solutio

ProLab 1000 What to do if...81ba75576e05 11/2013CalClock flashes6.2 ISE measurementError message Err1Obviously incorrectmeasured valuesError message,

What to do if... ProLab 100082ba75576e05 11/2013Warning [TempErr] Warning [ISEErr] 6.3 General errorsMeter does not reactto keystrokeTime is lostCause

ProLab 1000 Technical data83ba75576e05 11/2013Stand March 3, 2010Translation of the legally binding German version7 Technical data7.1 General dataDime

Technical data ProLab 100084ba75576e05 11/2013Stand March 3, 2010Translation of the legally binding German version7.2 Measuring ranges, resolution, ac

ProLab 1000 Technical data85ba75576e05 11/2013Stand March 3, 2010Translation of the legally binding German version7.2.2 ISENoteThe measuring ranges an

Technical data ProLab 100086ba75576e05 11/2013Stand March 3, 2010Translation of the legally binding German versionFCC Class A Equipment StatementNote:

ProLab 1000 Lists87ba75576e05 11/20138ListsThis chapter provides additional information and orientation aids.Abbreviations The list of abbreviations e

Lists ProLab 100088ba75576e05 11/2013Abbreviations°C Temperature unit, degrees Celsius°F Temperature unit, degrees FahrenheitCal Automatic calibration

ProLab 1000 Lists89ba75576e05 11/2013GlossaryAdjusting To manipulate a measuring system so that the relevant value (e. g. the displayed value) differs

ProLab 1000 Overview9ba75576e05 11/20131.3 DisplayThe graphic display displays the measurement data. The illumination enables to read the display even

Lists ProLab 100090ba75576e05 11/2013Potentiometry Name of a measuring technique. The signal (depending on the measured parameter) of the electrode is

ProLab 1000 Lists91ba75576e05 11/2013Trademarks usedTrademark Owner of the trademarkBaker Mallinckrodt Baker, Inc.Beckman Beckman Instruments, Inc.Fis

Lists ProLab 100092ba75576e05 11/2013

ProLab 1000 Index 93ba75576e05 11/2013AAuthorized use ...15BBattery compartment ...

Index ProLab 100094ba75576e05 11/2013Single-point calibrationpH ... 48SlopeISE ...

ProLab 100095ba75576e05 11/2013AppendixA.1 Firmware updateGeneral information With the Update_ProLab1000_2000 program and a PC you can update the firm

ProLab 100096ba75576e05 11/2013After switching the meter off and on you can check whether the meter has taken over the new software version.8 Disconne

ProLab 100097ba75576e05 11/2013A.2 MenusA.2.1 Data storageStorage & config (<MENU/OK_>)– Data storage– Manual data storage (<RCL>)– Di

ProLab 100098ba75576e05 11/2013A.2.2 DisplayA.2.3 SystemStorage & config (<MENU/OK_>)– Data storage (see page 97)– Display– Time : On /Off–

ProLab 100099ba75576e05 11/2013A.2.4 <STO_>A.2.5 <PRT_><STO_> (<STO_>)– SAMPLE ID : 1 ... 999– Interval : 1, 5 s, 10 s, 30 s,